Subsections
[Cr:4, Lc:3, Tt:0, Lb:0]
Knowledge of the content of CHM602 is essential to follow this course.
- Magic angle spinning (MAS) NMR: Magic angle spinning experiments.
Theoretical description of MAS via Wigner rotation matrices, the
concept of powder averaging. Representation of spin interactions
through second rank tensors.
- Recoupling experiments in SSNMR: Selective and broadband recoupling
techniques. Gamma and non-gamma encoded sequences. Homonuclear and
heteronuclear recoupling experiments and examples. Polarization
transfer experiments in the solid sate, spectral assignment
experiments, distance and torsion angle experiments.
- Decoupling experiments in SSNMR: Homonuclear and heteronuclear
decoupling experiments, broadband and selective decoupling experiments
and examples.
- K. Schmidt-Rohr, H. Spiess, Multi-dimensional Solid-state NMR
and Polymers, 1st Ed, Academic Press, London (1996).
- M. Mehring, High Resolution NMR of Solids, 1st Ed, Springer,
New York (1975).
- U. Haeberlen, High Resolution NMR of Solids: Advances in
Magnetic Resonances: Supplement I, 1st Ed, Academic Press, San Diego
(1976).
- B. C. Gerstein, C. R. Dybowski, Transient Techniques in NMR of
Solid, 1st Ed, Academic Press, Orlando (1985).
