Subsections
[Cr:4, Lc:3, Tt:0, Lb:0]
Knowledge of the content of CHM301/PHY302, CHM402/PHY403 is essential to follow this course.
- Introduction to NMR: Spin and spin angular momentum, CW NMR, pulse
NMR, sampling, bandwidth, detection and acquisition of NMR signals,
time and frequency domain spectra, FT-NMR, resolution and sensitivity
in NMR.
- Spin interactions in NMR, chemical shift, scalar or J-coupling,
dipolar interaction and quadrupole interaction, quantum mechanical
description of spin-interactions, spin interactions in the solution
and solid-state.
- Pulse NMR experiments, describing pulse NMR experiment: The
radio-frequency field, pulse, the concept of rotating frame,
relaxation, spin-lattice relaxation, spin-spin relaxation, nuclear
overhauser effect (NOE).
- Polarization transfer experiments and spectrum editing, selecting
polarization transfer, INEPT experiment, implementation and its
Characteristics, DEPT experiment, implementation and its
characteristics, cross-polarization (CP) experiment and its variants.
- Fourier transform NMR, single-pulse experiment, signal averaging,
multiple-pulse NMR experiments, NMR spectrum, NMR signal, line shapes
in NMR, two-dimensional NMR spectroscopy, two-dimensional fourier
transformation.
- R. S. Macomber, A Complete introduction to modern NMR
techniques, 1st Ed, John Wiley & Sons, England (1998).
- M. H. Levitt, Spin dynamics: Basics of Nuclear Magnetic
Resonance, 2nd Ed, John Wiley & Sons, England (2008).
- C. P. Slichter, Principles of Magnetic Resonance, 3rd Ed,
Springer Verlag, Berlin (1996).
